3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole

Base Information

Chemical Name:3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole
CAS No.:156606-81-4
Molecular Formula:C₁₆H₁₁F₆OSb
Molecular Weight:455.003
Hs Code.:

Synonyms:3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole

Suppliers and Price of 3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole

There total 1 articles about 3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 70091-67-7
lithium 1,1,1,3,3,3-hexafluoro-2-(2-lithiophenyl)-2-propoxide

: 87856-09-5
dichloro(4-methylphenyl)stibine

: 156606-81-4
3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole

Guidance literature:: With H₂O; In tetrahydrofuran; -78°C, stirring (room temp., 12 h), water quenching; column chromy. (n-hexane/ethyl acetate); elem. anal.;

Reference yield: 100.0%

: 7791-25-5
sulfuryl dichloride

: 156606-81-4
3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole

: 1,1-dichloro-3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-benzoxastibole

Guidance literature:: In dichloromethane; N2-atmosphere; stirring (room temp., 1 h); evapn. (reduced pressure);
DOI:10.1021/om00004a053

Reference yield:

: 156606-81-4
3,3-bis(trifluoromethyl)-1-(4-methylphenyl)-3H-2,1-banzoxastibole

: 3,3,3'-tris(trifluoromethyl)-3'-methyl-1-(4-methylphenyl)-1,1'-spirobi(3H-2,1-benzoxastibole)

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: n-BuLi; NH₄Cl / water; tetrahydrofuran; diethyl ether

With n-BuLi; NH₄Cl; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/om00004a053