1-(3-{[4-(2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}phenyl)methanesulfonamide

Base Information

Chemical Name:1-(3-{[4-(2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}phenyl)methanesulfonamide
CAS No.:1335490-37-3
Molecular Formula:C₁₇H₁₇N₅O₃S
Molecular Weight:371.42
Hs Code.:

Synonyms:1-(3-{[4-(2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}phenyl)methanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3-{[4-(2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}phenyl)methanesulfonamide

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Technology Process of 1-(3-{[4-(2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}phenyl)methanesulfonamide

There total 2 articles about 1-(3-{[4-(2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}phenyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

: 1335490-10-2
3-[(4-chloro-1,3,5-triazin-2-yl)amino]benzenemethanesulfonamide

: 5720-06-9
2-Methoxyphenylboronic acid

: 1335490-37-3
1-(3-{[4-(2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}phenyl)methanesulfonamide

Guidance literature:: With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; water; at 140 ℃; for 1h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 344750-15-8
(3-aminophenyl)methanesulfonamide

: 1335490-37-3
1-(3-{[4-(2-methoxyphenyl)-1,3,5-triazin-2-yl]amino}phenyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 2.5 h / 0 °C / Inert atmosphere

2: potassium phosphate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 1 h / 140 °C / Inert atmosphere; Microwave irradiation

With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; water; N,N-dimethyl-formamide;