7-amino-3-methyl-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole hydrochloride

Base Information

Chemical Name:7-amino-3-methyl-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole hydrochloride
CAS No.:134541-23-4
Molecular Formula:C₁₇H₁₆N₂O₂*ClH
Molecular Weight:316.787
Hs Code.:

7-amino-3-methyl-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopenta<f>benzoxazole hydrochloride

Synonyms:7-amino-3-methyl-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-amino-3-methyl-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole hydrochloride

Chemical Property:

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Technology Process of 7-amino-3-methyl-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole hydrochloride

There total 2 articles about 7-amino-3-methyl-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 134541-21-2
3-methyl-7-oximino-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole

: 134541-23-4
7-amino-3-methyl-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole hydrochloride

Guidance literature:: With hydrogen; nickel; In methanol; at 80 ℃; for 7h; under 36200.4 Torr;

Reference yield:

: 80428-00-8
2,7-dioxo-3-methyl-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole

: 134541-23-4
7-amino-3-methyl-2-oxo-5-phenyl-2,3,5,6-tetrahydrocyclopentabenzoxazole hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NH₂OH*HCl, NaOAc / ethanol / 6 h / Heating

2: 54 percent / H₂ / Raney-Ni / methanol / 7 h / 80 °C / 36200.4 Torr

With hydroxylamine hydrochloride; hydrogen; sodium acetate; nickel; In methanol; ethanol;