N-t-butyloxycarbonyl-N’-(2-methyldec-5-yn-4-yl)-N’-p-toluenesulfonylhydrazine

Base Information

• Chemical Name: N-t-butyloxycarbonyl-N’-(2-methyldec-5-yn-4-yl)-N’-p-toluenesulfonylhydrazine
• CAS No.: 1415714-56-5
• Molecular Formula: C₂₃H₃₆N₂O₄S
• Molecular Weight: 436.616
• Mol file: 1415714-56-5.mol

Synonyms:N-t-butyloxycarbonyl-N’-(2-methyldec-5-yn-4-yl)-N’-p-toluenesulfonylhydrazine

Chemical Property of N-t-butyloxycarbonyl-N’-(2-methyldec-5-yn-4-yl)-N’-p-toluenesulfonylhydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-t-butyloxycarbonyl-N’-(2-methyldec-5-yn-4-yl)-N’-p-toluenesulfonylhydrazine

There total 2 articles about N-t-butyloxycarbonyl-N’-(2-methyldec-5-yn-4-yl)-N’-p-toluenesulfonylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

tert-butyl 2-tosylhydrazine-1-carboxylate (260788-12-3) + 2-methyldec-5-yn-4-ol (627526-24-3) → N-t-butyloxycarbonyl-N’-(2-methyldec-5-yn-4-yl)-N’-p-toluenesulfonylhydrazine (1415714-56-5)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; regiospecific reaction; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.10.084

Reference yield: 78.0%

5-methyl-1-phenyl-1-hexyn-3-ol (15212-29-0) + tert-butyl 2-tosylhydrazine-1-carboxylate (260788-12-3) → N-t-butyloxycarbonyl-N’-(2-methyldec-5-yn-4-yl)-N’-p-toluenesulfonylhydrazine (1415714-56-5)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; regiospecific reaction; Inert atmosphere;

DOI:10.1016/j.tetlet.2012.10.084

upstream raw materials:

tert-butyl 2-tosylhydrazine-1-carboxylate

2-methyldec-5-yn-4-ol

5-methyl-1-phenyl-1-hexyn-3-ol