(2S,3S)-3-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-methyl-2-(4-methylpent-3-en-1-yl)oxirane

Base Information

Chemical Name:(2S,3S)-3-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-methyl-2-(4-methylpent-3-en-1-yl)oxirane
CAS No.:1415456-09-5
Molecular Formula:C₂₃H₃₆O₃
Molecular Weight:360.537
Hs Code.:

Synonyms:(2S,3S)-3-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-methyl-2-(4-methylpent-3-en-1-yl)oxirane

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Chemical Property of (2S,3S)-3-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-methyl-2-(4-methylpent-3-en-1-yl)oxirane

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Technology Process of (2S,3S)-3-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-methyl-2-(4-methylpent-3-en-1-yl)oxirane

There total 3 articles about (2S,3S)-3-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-methyl-2-(4-methylpent-3-en-1-yl)oxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: C₁₀H₁₇BrO

: 1415456-08-4
1,5-dimethoxy-6-(3-methylbut-2-en-1-yl)cyclohexa-1,4-diene

: 1415456-09-5
(2S,3S)-3-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-methyl-2-(4-methylpent-3-en-1-yl)oxirane

Guidance literature:: 1,5-dimethoxy-6-(3-methylbut-2-en-1-yl)cyclohexa-1,4-diene; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 - 30 ℃; for 1h;

C₁₀H₁₇BrO; In tetrahydrofuran; cyclohexane; at -78 - -10 ℃; for 2.25h;

Reference yield:

: 37567-78-5
1,5-dimethoxy-1,4-cyclohexadiene

: 1415456-09-5
(2S,3S)-3-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-methyl-2-(4-methylpent-3-en-1-yl)oxirane

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium; barium(II) iodide / pentane; tetrahydrofuran / 1 h / -78 °C

1.2: 2.25 h

2.1: sec.-butyllithium / cyclohexane; tetrahydrofuran / 1 h / -78 - 30 °C

2.2: 2.25 h / -78 - -10 °C

With barium(II) iodide; tert.-butyl lithium; sec.-butyllithium; In tetrahydrofuran; cyclohexane; pentane;

Reference yield:

: 503-60-6
3,3-dimethyl-allyl chloride

: 1415456-09-5
(2S,3S)-3-((2,6-dimethoxy-1-(3-methylbut-2-en-1-yl)cyclohexa-2,5-dien-1-yl)methyl)-2-methyl-2-(4-methylpent-3-en-1-yl)oxirane

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butyl lithium; barium(II) iodide / pentane; tetrahydrofuran / 1 h / -78 °C

1.2: 2.25 h

2.1: sec.-butyllithium / cyclohexane; tetrahydrofuran / 1 h / -78 - 30 °C

2.2: 2.25 h / -78 - -10 °C

With barium(II) iodide; tert.-butyl lithium; sec.-butyllithium; In tetrahydrofuran; cyclohexane; pentane;