tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate

Base Information

Chemical Name:tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate
CAS No.:1083003-48-8
Molecular Formula:C₁₆H₂₁N₅O₄S
Molecular Weight:379.44
Hs Code.:

Synonyms:tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate

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Technology Process of tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate

There total 1 articles about tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1083003-47-7
C₁₆H₂₁N₅O₂S

: 1083003-48-8
tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In methanol; water; at 20 ℃; for 1h;
DOI:10.1055/s-2008-1078011

Reference yield: 94.0%

: 1083003-48-8
tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 121030-25-9
(2E)-1--4-cyclohexylidene-2-butene

Guidance literature:: tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃;

cyclohexanone; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1055/s-2008-1078011

Reference yield: 59.0%

: 1083003-48-8
tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate

: 104-55-2
3-phenyl-propenal

: C₁₈H₂₃NO₂

Guidance literature:: tert-butyl (E)-4-(1-phenyl-1H-tetrazol-5-ylsulfonyl)but-2-enyl carbamate; With 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃;

3-phenyl-propenal; In tetrahydrofuran; toluene; at -78 - 20 ℃; optical yield given as %de;
DOI:10.1055/s-2008-1078011