[Pd(C,N-C₆H₂CH₂CH₂NH₂-6,(OMe)2-3,4)(N,N,N',N'-tetramethylethylenediamine)]Br

Base Information

Chemical Name:[Pd(C,N-C₆H₂CH₂CH₂NH₂-6,(OMe)2-3,4)(N,N,N',N'-tetramethylethylenediamine)]Br
CAS No.:1372870-55-7
Molecular Formula:Br*C₁₆H₃₀N₃O₂Pd
Molecular Weight:482.757
Hs Code.:

[Pd(C,N-C<sub>6</sub>H<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>NH<sub>2</sub>-6,(OMe)2-3,4)(N,N,N',N'-tetramethylethylenediamine)]Br

Synonyms:[Pd(C,N-C₆H₂CH₂CH₂NH₂-6,(OMe)2-3,4)(N,N,N',N'-tetramethylethylenediamine)]Br

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Chemical Property of [Pd(C,N-C₆H₂CH₂CH₂NH₂-6,(OMe)2-3,4)(N,N,N',N'-tetramethylethylenediamine)]Br

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Technology Process of [Pd(C,N-C₆H₂CH₂CH₂NH₂-6,(OMe)2-3,4)(N,N,N',N'-tetramethylethylenediamine)]Br

There total 1 articles about [Pd(C,N-C₆H₂CH₂CH₂NH₂-6,(OMe)2-3,4)(N,N,N',N'-tetramethylethylenediamine)]Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 63375-81-5
2-(2-bromo-4,5-dimethoxyphenylphenyl)ethan-1-amine

: 32005-36-0
bis(dibenzylideneacetone)-palladium⁽⁰⁾

: 1372870-55-7
[Pd(C,N-C₆H₂CH₂CH₂NH₂-6,(OMe)2-3,4)(N,N,N',N'-tetramethylethylenediamine)]Br

Guidance literature:: In toluene; byproducts: Pd; diamine was added to suspn. of Pd compd. in toluene; stirred for 10 min under N2; amine was added; stirred for 24 h; filtered; washed (Et2O); air-dried; elem. anal.;
DOI:10.1021/om300141b

Reference yield: 58.0%

: 1372870-55-7
[Pd(C,N-C₆H₂CH₂CH₂NH₂-6,(OMe)2-3,4)(N,N,N',N'-tetramethylethylenediamine)]Br

: 603-35-0
triphenylphosphine

: 1372870-45-5
[Pd(C,N-C₆H₂CH₂CH₂NH₂-6,(OMe)2-3,4)Br(PPh₃)]

Guidance literature:: In dichloromethane; PPh3 (1 equiv.) was added to suspn. of Pd complex in CH2Cl2; stirred for3 h; filtered through MgSO4; concd.; Et2O added; filtered; washed (Et2O); air-dried; elem. anal.;
DOI:10.1021/om300141b