phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside

Base Information

• Chemical Name: phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside
• CAS No.: 169236-77-5
• Molecular Formula: C₂₈H₂₆O₈
• Molecular Weight: 490.51
• Mol file: 169236-77-5.mol

Synonyms:phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside

Chemical Property of phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside

There total 1 articles about phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

1,2-Di-O-acetyl-3,5-di-O-benzoyl-6-desoxy-D-glucofuranose (122331-59-3) + phenol (108-95-2,27073-41-2) → phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside (169236-77-5) + phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-α-D-glucofuranoside

Guidance literature:

With tin(IV) chloride; In toluene; for 15h;

DOI:10.1016/0040-4020(95)00262-7

Reference yield: 78.0%

phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside (169236-77-5) → phenyl 3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside

Guidance literature:

With sodium ethanolate; phenol; In ethanol; 1.) rt., 20 min.; 2.) 30 min.;

DOI:10.1016/0040-4020(95)00262-7

Reference yield: 75.0%

phenyl 2-O-acetyl-3,5-di-O-benzoyl-6-deoxy-β-D-glucofuranoside (169236-77-5) → phenyl 6-deoxy-β-D-glucofuranoside

Guidance literature:

With sodium methylate; In methanol; for 1h;

DOI:10.1016/0040-4020(95)00262-7

upstream raw materials:

1,2-Di-O-acetyl-3,5-di-O-benzoyl-6-desoxy-D-glucofuranose

phenol