N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride

Base Information

• Chemical Name: N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride
• CAS No.: 5180-19-8
• Molecular Formula: C₇H₄Cl₃NS
• Molecular Weight: 240.54
• Mol file: 5180-19-8.mol

Synonyms:N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride

Chemical Property of N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride

There total 2 articles about N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Chlorophenyl isothiocyanate (2131-55-7) → N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride (5180-19-8)

Guidance literature:

With chlorine; In chloroform;

DOI:10.1021/jo01341a046

Reference yield:

→ C7H4Cl3NS (5180-19-8)

Guidance literature:

entspr. RNCS, Cl2;

Reference yield: 69.0%

4-(2',3',4',6'-tetra-O-acetyl-β-D-glucopyranosyl)-3-thiosemicarbazide (63128-98-3) + N-(4-chloro-phenyl)-carbonochloridimidic hypochlorous thioanhydride (5180-19-8) → 3-(tetra-O-acetyl-β-D-glucopyranosylimino)-6-(4-chlorophenyl)imino-3,4,5,6-tetrahydro-1,2,4,5-dithiadiazine

Guidance literature:

In chloroform; for 3h; Reflux;

upstream raw materials:

4-Chlorophenyl isothiocyanate

Downstream raw materials:

5-(4-chloro-anilino)-[1,2,4]dithiazole-3-thione

4-(4-chloro-phenyl)-5-(4-chloro-phenylimino)-[1,2,4]dithiazolidine-3-thione

5-(4-chloro-phenylimino)-4-phenyl-[1,2,4]dithiazolidine-3-thione

4-phenyl-5-phenylimino-3-thio-1,2,4-thiadiazolidine