N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindol-4-yl>-N-methyl-3-furancarboxamide

Base Information

Chemical Name:N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindol-4-yl>-N-methyl-3-furancarboxamide
CAS No.:89651-06-9
Molecular Formula:C₂₄H₂₂N₂O₅S
Molecular Weight:450.515
Hs Code.:

N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenz<cd>indol-4-yl>-N-methyl-3-furancarboxamide

Synonyms:N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindol-4-yl>-N-methyl-3-furancarboxamide

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Chemical Property of N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindol-4-yl>-N-methyl-3-furancarboxamide

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Technology Process of N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindol-4-yl>-N-methyl-3-furancarboxamide

There total 6 articles about N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindol-4-yl>-N-methyl-3-furancarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124465-55-0,51867-05-1
1-benzoyl-1,2,2a,3-tetrahydro-benz[cd]indole

: 89651-06-9
N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindol-4-yl>-N-methyl-3-furancarboxamide

Guidance literature:: Multi-step reaction with 6 steps

1: conc. hydrochloric acid / 8 h / Heating

2: triethylamine / benzene / 5 h / Heating

3: 90 percent / m-chloroperbenzoic acid / CHCl₃ / 3 h / 5 °C

4: 93 percent / p-toluenesulfonic acid / toluene / 1 h / Heating

5: toluene / 6 h / Heating

6: triethylamine / toluene; benzene / 2 h / Heating

With hydrogenchloride; toluene-4-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In chloroform; toluene; benzene;
DOI:10.1248/cpb.39.23

Reference yield:

: 1,2,2a,3-Tetrahydro-benzo[cd]indole

: 89651-06-9
N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindol-4-yl>-N-methyl-3-furancarboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / benzene / 5 h / Heating

2: 90 percent / m-chloroperbenzoic acid / CHCl₃ / 3 h / 5 °C

3: 93 percent / p-toluenesulfonic acid / toluene / 1 h / Heating

4: toluene / 6 h / Heating

5: triethylamine / toluene; benzene / 2 h / Heating

With toluene-4-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In chloroform; toluene; benzene;
DOI:10.1248/cpb.39.23

Reference yield:

: 134745-86-1
1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindole

: 89651-06-9
N-<1-<(4-Methoxyphenyl)sulfonyl>-1,2,2a,3-tetrahydrobenzindol-4-yl>-N-methyl-3-furancarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / m-chloroperbenzoic acid / CHCl₃ / 3 h / 5 °C

2: 93 percent / p-toluenesulfonic acid / toluene / 1 h / Heating

3: toluene / 6 h / Heating

4: triethylamine / toluene; benzene / 2 h / Heating

With toluene-4-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In chloroform; toluene; benzene;
DOI:10.1248/cpb.39.23