1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride

Base Information

Chemical Name:1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride
CAS No.:1041752-86-6
Molecular Formula:C₂₅H₃₄N*Cl
Molecular Weight:384.005
Hs Code.:

Synonyms:1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride

Suppliers and Price of 1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride

There total 5 articles about 1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1070859-44-7
C₂₅H₃₃N

: 1041752-86-6
1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; toluene; at -10 - 50 ℃; Inert atmosphere; Schlenk technique;

Reference yield:

: 34713-70-7
2-Phenylpropanal

: 1041752-86-6
1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide; tetra-(n-butyl)ammonium iodide / toluene; water / 4 h / 60 °C

2: toluene / 4 h / Reflux

3: hydrogenchloride / toluene; 1,4-dioxane / -10 - 50 °C / Inert atmosphere; Schlenk technique

With hydrogenchloride; tetra-(n-butyl)ammonium iodide; sodium hydroxide; In 1,4-dioxane; water; toluene;

Reference yield:

: N-(2,6-diisopropylphenyl)-2-phenylpropan-1-imine

: 1041752-86-6
1-(2,6-diisopropylphenyl)-2,2,4-trimethyl-4-phenyl-3,4-dihydro-2H-pyrrol-1-ylium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 3.25 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

1.2: 12.25 h / -78 - 20 °C / Inert atmosphere; Schlenk technique

2.1: hydrogenchloride / diethyl ether / 0 - 90 °C / Inert atmosphere; Schlenk technique

With hydrogenchloride; n-butyllithium; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jacs.0c10705