2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde

Base Information

Chemical Name:2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde
CAS No.:1266327-42-7
Molecular Formula:C₂₄H₁₉F₃N₄O₂
Molecular Weight:452.436
Hs Code.:

Synonyms:2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde

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Chemical Property of 2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde

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Technology Process of 2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde

There total 1 articles about 2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-91-8,99108-56-2
morpholine

: C₂₁H₁₄F₃N₃O₃S

: 1266327-42-7
2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde

Guidance literature:: In dichloromethane; at 20 ℃; for 8h;
DOI:10.1016/j.tet.2010.11.073

Reference yield: 86.0%

: 1266327-42-7
2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde

: 2365-48-2
Methyl thioglycolate

: 1266327-57-4
6-methoxycarbonyl-2-morpholino-7-phenyl-4-(3-trifluoromethylanilino)quinazoline

Guidance literature:: Methyl thioglycolate; With potassium; In methanol;

2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde; In methanol; Microwave irradiation;
DOI:10.1016/j.tet.2010.11.073

Reference yield: 48.0%

: 1266327-42-7
2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde

: 2365-48-2
Methyl thioglycolate

: 1266327-56-3
methyl (Z)-2-[5-formyl-2-morpholino-6-(3-trifluoromethylanilino)-4-pyrimidinyl-1-phenyl-ethenyl]thioacetate

Guidance literature:: Methyl thioglycolate; With potassium; In methanol;

2-morpholino-6-phenylethynyl-4-(3-trifluoromethylanilino)pyrimidine-5-carbaldehyde; In methanol; Reflux;
DOI:10.1016/j.tet.2010.11.073