tert-butyl (1R,2R)-3-(allyloxycarbonyloxy)-1-hydroxy-1-phenylpropan-2-ylcarbamate

Base Information

Chemical Name:tert-butyl (1R,2R)-3-(allyloxycarbonyloxy)-1-hydroxy-1-phenylpropan-2-ylcarbamate
CAS No.:1132645-27-2
Molecular Formula:C₁₈H₂₅NO₆
Molecular Weight:351.4
Hs Code.:

Synonyms:tert-butyl (1R,2R)-3-(allyloxycarbonyloxy)-1-hydroxy-1-phenylpropan-2-ylcarbamate

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Chemical Property of tert-butyl (1R,2R)-3-(allyloxycarbonyloxy)-1-hydroxy-1-phenylpropan-2-ylcarbamate

Chemical Property:

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Technology Process of tert-butyl (1R,2R)-3-(allyloxycarbonyloxy)-1-hydroxy-1-phenylpropan-2-ylcarbamate

There total 3 articles about tert-butyl (1R,2R)-3-(allyloxycarbonyloxy)-1-hydroxy-1-phenylpropan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 2937-50-0
Allyl chloroformate

: 1009093-14-4
((1R,2R)-2-hydroxy-1-hydroxymethyl-2-phenylethyl)carbamic acid tert-butyl ester

: 1132645-27-2
tert-butyl (1R,2R)-3-(allyloxycarbonyloxy)-1-hydroxy-1-phenylpropan-2-ylcarbamate

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 0.35h;
DOI:10.1021/jo802611t

Reference yield:

: 46032-98-8
(1R,2R)-2-amino-1-phenylpropane-1,3-diol

: 1132645-27-2
tert-butyl (1R,2R)-3-(allyloxycarbonyloxy)-1-hydroxy-1-phenylpropan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 2 h / 20 °C

2: pyridine / dichloromethane / 1 h / 0 - 20 °C

With pyridine; In methanol; dichloromethane;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1132645-27-2
tert-butyl (1R,2R)-3-(allyloxycarbonyloxy)-1-hydroxy-1-phenylpropan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 2 h / 20 °C

2: pyridine / dichloromethane / 1 h / 0 - 20 °C

With pyridine; In methanol; dichloromethane;