4-{6-[5'-(N-butylcarbazole-3-yl)-2,2'-bithiophene-5-yl]-N-butylcarbazole-3-yl}-styrene

Base Information

Chemical Name:4-{6-[5'-(N-butylcarbazole-3-yl)-2,2'-bithiophene-5-yl]-N-butylcarbazole-3-yl}-styrene
CAS No.:1443044-26-5
Molecular Formula:C₄₈H₄₂N₂S₂
Molecular Weight:711.007
Hs Code.:

Synonyms:4-{6-[5'-(N-butylcarbazole-3-yl)-2,2'-bithiophene-5-yl]-N-butylcarbazole-3-yl}-styrene

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Chemical Property of 4-{6-[5'-(N-butylcarbazole-3-yl)-2,2'-bithiophene-5-yl]-N-butylcarbazole-3-yl}-styrene

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Technology Process of 4-{6-[5'-(N-butylcarbazole-3-yl)-2,2'-bithiophene-5-yl]-N-butylcarbazole-3-yl}-styrene

There total 4 articles about 4-{6-[5'-(N-butylcarbazole-3-yl)-2,2'-bithiophene-5-yl]-N-butylcarbazole-3-yl}-styrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1443044-23-2
4-[6-(4,4,5,5-tetramethyl-1,3,2-dioxaboroyl)-N-butylcarbazole-3-yl]-styrene

: 1443044-24-3
C₂₄H₂₀BrNS₂

: 1443044-26-5
4-{6-[5'-(N-butylcarbazole-3-yl)-2,2'-bithiophene-5-yl]-N-butylcarbazole-3-yl}-styrene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; at 60 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.polymer.2013.04.002

Reference yield:

: 121602-03-7
3,6-dibromo-(N-n-butyl)carbazole

: 1443044-26-5
4-{6-[5'-(N-butylcarbazole-3-yl)-2,2'-bithiophene-5-yl]-N-butylcarbazole-3-yl}-styrene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 24 h / 60 °C / Schlenk technique; Inert atmosphere

2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran / 24 h / 60 °C / Schlenk technique; Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 24 h / 60 °C / Schlenk technique; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; In tetrahydrofuran; water; 1: |Suzuki Coupling / 2: |Suzuki Coupling / 3: |Suzuki Coupling;
DOI:10.1016/j.polymer.2013.04.002

Reference yield:

: 2156-04-9,593231-72-2
4-Vinylphenylboronic acid

: 1443044-26-5
4-{6-[5'-(N-butylcarbazole-3-yl)-2,2'-bithiophene-5-yl]-N-butylcarbazole-3-yl}-styrene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 24 h / 60 °C / Schlenk technique; Inert atmosphere

2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran / 24 h / 60 °C / Schlenk technique; Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 24 h / 60 °C / Schlenk technique; Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium carbonate; In tetrahydrofuran; water; 1: |Suzuki Coupling / 2: |Suzuki Coupling / 3: |Suzuki Coupling;
DOI:10.1016/j.polymer.2013.04.002