Technology Process of 1,3-di-O-benzoyl-D-glycero-tetrulose
There total 6 articles about 1,3-di-O-benzoyl-D-glycero-tetrulose which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 56 percent / 1.) sodium hydride, 2.) tetrabutylammonium iodide / tetrahydrofuran / 3 h / Ambient temperature
2: 86 percent / sulfuric acid / 95 - 100 °C
3: pyridine / 168 h / Ambient temperature
4: 95 percent / molecular sieve 3A, pyridinium dichromate / CH2Cl2 / 8 h
5: 45 percent / 45 percent hydrogen bromide / acetic acid / 0.05 h
With
pyridine; dipyridinium dichromate; 3 A molecular sieve; sulfuric acid; hydrogen bromide; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1016/0008-6215(84)85254-4
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 86 percent / sulfuric acid / 95 - 100 °C
2: pyridine / 168 h / Ambient temperature
3: 95 percent / molecular sieve 3A, pyridinium dichromate / CH2Cl2 / 8 h
4: 45 percent / 45 percent hydrogen bromide / acetic acid / 0.05 h
With
pyridine; dipyridinium dichromate; 3 A molecular sieve; sulfuric acid; hydrogen bromide;
In
dichloromethane; acetic acid;
DOI:10.1016/0008-6215(84)85254-4
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / 168 h / Ambient temperature
2: 95 percent / molecular sieve 3A, pyridinium dichromate / CH2Cl2 / 8 h
3: 45 percent / 45 percent hydrogen bromide / acetic acid / 0.05 h
With
pyridine; dipyridinium dichromate; 3 A molecular sieve; hydrogen bromide;
In
dichloromethane; acetic acid;
DOI:10.1016/0008-6215(84)85254-4
