(1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ²(N,C)-(NHC(C₆H₅₎₂-2-C₆H₄)]

Base Information

Chemical Name:(1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ²(N,C)-(NHC(C₆H₅₎₂-2-C₆H₄)]
CAS No.:1027606-79-6
Molecular Formula:C₂₉H₃₀IrN
Molecular Weight:584.784
Hs Code.:

(1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ<sup>2</sup>(N,C)-(NHC(C<sub>6</sub>H<sub>5)2</sub>-2-C<sub>6</sub>H<sub>4</sub>)]

Synonyms:(1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ²(N,C)-(NHC(C₆H₅₎₂-2-C₆H₄)]

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Chemical Property of (1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ²(N,C)-(NHC(C₆H₅₎₂-2-C₆H₄)]

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Technology Process of (1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ²(N,C)-(NHC(C₆H₅₎₂-2-C₆H₄)]

There total 1 articles about (1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ²(N,C)-(NHC(C₆H₅₎₂-2-C₆H₄)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: Cp*IrCl[κ2(N,C)-(NH2C(C6H5)2-2-C6H4)]*0.5CH2Cl2

: 1027606-79-6
(1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ²(N,C)-(NHC(C₆H₅₎₂-2-C₆H₄)]

Guidance literature:: With t-BuOK; In dichloromethane; under Ar atm. mixt. Ir complex and t-BuOK in CH2Cl2 was stirred at room temp. for 21 h; solvent was removed in vacuo, residue was dissolved in Et2O, filtered and evapd. to drynes, recrystn. from Et2O; elem. anal.;
DOI:10.1021/om800124f

Reference yield: 88.0%

: 1027606-79-6
(1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ²(N,C)-(NHC(C₆H₅₎₂-2-C₆H₄)]

: 67-63-0,8013-70-5
isopropyl alcohol

: 1027606-81-0
[Cp*Ir(H){κ₂(N,C)-NH₂C(C₆H₅)₂-2-C₆H₄}]

Guidance literature:: In isopropyl alcohol; under Ar atm. Ir complex in 2-propanol was stirred at room temp. overnight; solvent was removed in vacuo, residue was washed with hexane and dried in vacuo; elem. anal.;
DOI:10.1021/om800124f

Reference yield: 87.0%

: 1027606-79-6
(1,2,3,4,5-pentamethylcyclopentadienyl)Ir-[κ²(N,C)-(NHC(C₆H₅₎₂-2-C₆H₄)]

: 67-64-1
acetone

: 1033052-09-3
Cp*Ir(CH2COCH3)[κ2(N,C)-(NH2C(C6H5)2-2-C6H4)]

Guidance literature:: In acetone; under Ar atm. soln. Ir complex in acetone was stirred at room temp. overnight; solvent was removed in vacuo, residue was washed with hexane and recrystd. from acetone; elem. anal.;
DOI:10.1021/om800124f