N¹-Benzyl-2-(2-benzylsulfanyl-ethyl)-2-[(thiophene-2-carbonyl)-amino]-succinamide

Base Information

• Chemical Name: N¹-Benzyl-2-(2-benzylsulfanyl-ethyl)-2-[(thiophene-2-carbonyl)-amino]-succinamide
• CAS No.: 201412-71-7
• Molecular Formula: C₂₅H₂₇N₃O₃S₂
• Molecular Weight: 481.64

Synonyms:N¹-Benzyl-2-(2-benzylsulfanyl-ethyl)-2-[(thiophene-2-carbonyl)-amino]-succinamide

Chemical Property of N¹-Benzyl-2-(2-benzylsulfanyl-ethyl)-2-[(thiophene-2-carbonyl)-amino]-succinamide

Chemical Property:

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Technology Process of N¹-Benzyl-2-(2-benzylsulfanyl-ethyl)-2-[(thiophene-2-carbonyl)-amino]-succinamide

There total 3 articles about N¹-Benzyl-2-(2-benzylsulfanyl-ethyl)-2-[(thiophene-2-carbonyl)-amino]-succinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[3-(Benzhydrylidene-amino)-2-oxo-tetrahydro-thiophen-3-yl]-acetic acid tert-butyl ester (201412-65-9) → N1-Benzyl-2-(2-benzylsulfanyl-ethyl)-2-[(thiophene-2-carbonyl)-amino]-succinamide (201412-71-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 90 percent / H₂O

2: 75 percent / aq. Na₂CO₃ / dioxane / Ambient temperature

With water; sodium carbonate; In 1,4-dioxane;

Reference yield:

(3-Amino-2-oxo-tetrahydro-thiophen-3-yl)-acetic acid; compound with trifluoro-acetic acid → N1-Benzyl-2-(2-benzylsulfanyl-ethyl)-2-[(thiophene-2-carbonyl)-amino]-succinamide (201412-71-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / aq. Na₂CO₃ / dioxane / Ambient temperature

With sodium carbonate; In 1,4-dioxane;

Reference yield:

thiophen-2-carboxylic anhydride (25569-97-5) + benzyl bromide (100-39-0) + benzylamine (100-46-9) + (3-Allyloxycarbonylamino-2-oxo-tetrahydro-thiophen-3-yl)-acetic acid (201412-68-2) → N1-Benzyl-2-(2-benzylsulfanyl-ethyl)-2-[(thiophene-2-carbonyl)-amino]-succinamide (201412-71-7)

Guidance literature:

Multistep reaction;

upstream raw materials:

thiophen-2-carboxylic anhydride

benzyl bromide

benzylamine

(3-Allyloxycarbonylamino-2-oxo-tetrahydro-thiophen-3-yl)-acetic acid

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