C₂₆H₄₂N₆

Base Information

• Chemical Name: C₂₆H₄₂N₆
• CAS No.: 1402397-29-8
• Molecular Formula: C₂₆H₄₂N₆
• Molecular Weight: 438.66
• Mol file: 1402397-29-8.mol

Synonyms:C₂₆H₄₂N₆

Chemical Property of C₂₆H₄₂N₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₄₂N₆

There total 3 articles about C₂₆H₄₂N₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

C42H46N6O4 (1402397-28-7) → C26H42N6 (1402397-29-8)

Guidance literature:

With hydrazine hydrate; In tetrahydrofuran; ethanol; at 80 ℃; for 15h; Inert atmosphere;

DOI:10.1021/ic301506x

Reference yield:

2-(3-(hydroxymethyl)phenyl)isoindoline-1,3-dione (92789-55-4) → C26H42N6 (1402397-29-8)

Guidance literature:

Multi-step reaction with 3 steps

1: triphenylphosphine; carbon tetrabromide / dichloromethane / 2 h / -5 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetonitrile / 60 h / Reflux; Inert atmosphere

3: hydrazine hydrate / tetrahydrofuran; ethanol / 15 h / 80 °C / Inert atmosphere

With carbon tetrabromide; potassium carbonate; hydrazine hydrate; triphenylphosphine; potassium iodide; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;

DOI:10.1021/ic301506x

Reference yield:

N-(3-Bromomethylphenyl)phthalimide (129747-78-0) → C26H42N6 (1402397-29-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetonitrile / 60 h / Reflux; Inert atmosphere

2: hydrazine hydrate / tetrahydrofuran; ethanol / 15 h / 80 °C / Inert atmosphere

With potassium carbonate; hydrazine hydrate; potassium iodide; In tetrahydrofuran; ethanol; acetonitrile;

DOI:10.1021/ic301506x

upstream raw materials:

2-(3-(hydroxymethyl)phenyl)isoindoline-1,3-dione

N-(3-Bromomethylphenyl)phthalimide

C₄₂H₄₆N₆O₄