(S)-5-(benzyloxy)hept-1-ene

Base Information

Chemical Name:(S)-5-(benzyloxy)hept-1-ene
CAS No.:1392302-18-9
Molecular Formula:C₁₄H₂₀O
Molecular Weight:204.312
Hs Code.:

Synonyms:(S)-5-(benzyloxy)hept-1-ene

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Chemical Property of (S)-5-(benzyloxy)hept-1-ene

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Technology Process of (S)-5-(benzyloxy)hept-1-ene

There total 2 articles about (S)-5-(benzyloxy)hept-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1392302-28-1
(R)-3-(benzyloxy)hept-6-en-1-yl p-toluenesulfonate

: 1392302-18-9
(S)-5-(benzyloxy)hept-1-ene

Guidance literature:: (R)-3-(benzyloxy)hept-6-en-1-yl p-toluenesulfonate; With lithium triethylborohydride; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; water;
DOI:10.1016/j.tetasy.2012.06.009

Reference yield:

: C₃₀H₃₈O₂Si

: 1392302-18-9
(S)-5-(benzyloxy)hept-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 62 h / 20 °C / Inert atmosphere

2: pyridine / 15 h / 0 °C / Inert atmosphere

3: lithium triethylborohydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

With pyridine; tetrabutyl ammonium fluoride; lithium triethylborohydride; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2012.06.009

Reference yield:

: 1392302-18-9
(S)-5-(benzyloxy)hept-1-ene

: C₃₇H₃₈O₅

Guidance literature:: Multi-step reaction with 2 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 45 °C / Inert atmosphere

2: lithium tetrafluoroborate / water; acetonitrile / 1 h / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium tetrafluoroborate; In dichloromethane; water; acetonitrile;
DOI:10.1016/j.tetasy.2012.06.009