benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

Base Information

• Chemical Name: benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside
• CAS No.: 155780-03-3
• Molecular Formula: C₃₃H₄₄N₂O₁₃
• Molecular Weight: 676.718

Synonyms:benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

Chemical Property of benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

There total 1 articles about benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + [(2S,3R,4R,5S,6R)-3-Acetylamino-5-((2S,3R,4R,5S,6R)-3-acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-2-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-4-yloxy]-acetic acid → benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside (155780-03-3)

Guidance literature:

In methanol; at 0 ℃; for 0.5h; Yield given;

DOI:10.1016/0008-6215(94)84291-4

Reference yield: 73.0%

2,2-dimethoxy-propane (77-76-9) + benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside (155780-03-3) → benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

Guidance literature:

With trifluorormethanesulfonic acid; In acetone; for 6h; Ambient temperature;

DOI:10.1016/0008-6215(94)84291-4

Reference yield: 65.0%

acetic anhydride (108-24-7) + benzyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside (155780-03-3) → benzyl 2-acetamido-4-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-6-O-benzyl-2-deoxy-3-O-(methoxycarbonyl)methyl-α-D-glucopyranoside

Guidance literature:

With pyridine; for 12h; Ambient temperature;

DOI:10.1016/0008-6215(94)84291-4

upstream raw materials:

diazomethane

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