(2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester

Base Information

Chemical Name:(2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester
CAS No.:940055-72-1
Molecular Formula:C₂₇H₂₅N₃O₆
Molecular Weight:487.512
Hs Code.:

Synonyms:(2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester

Suppliers and Price of (2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester

There total 3 articles about (2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 940055-59-4
3-(2-amino-benzylamino)-pyrrolidine-2,5-dione

: 940055-72-1
(2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester

Guidance literature:: dmap; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 28144-70-9,88-68-6
anthranilic acid amide

: 940055-72-1
(2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylsulfide borane complex / tetrahydrofuran / 8 h / Heating / reflux

2: ethyl acetate / 20 - 70 h / 20 - 50 °C

3: dmap / tetrahydrofuran / 20 °C

With dimethylsulfide borane complex; dmap; In tetrahydrofuran; ethyl acetate;

Reference yield:

: 4403-69-4
2-amino-1-benzylamine

: 940055-72-1
(2-{[benzyloxycarbonyl-(2,5-dioxopyrrolidin-3-yl)amino]methyl}-phenyl)carbamoyl acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: ethyl acetate / 20 - 70 h / 20 - 50 °C

2: dmap / tetrahydrofuran / 20 °C

dmap; In tetrahydrofuran; ethyl acetate;