Technology Process of C22H28FNO5S
There total 10 articles about C22H28FNO5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H28FNO3S;
With
potassium carbonate;
In
ethanol; water; acetonitrile;
at 5 ℃;
With
dihydrogen peroxide;
In
ethanol; water; acetonitrile;
for 1h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: aluminum (III) chloride / 16 h / 20 °C / Reflux
2.1: potassium carbonate; tetrabutylammomium bromide / toluene / 24 h / Reflux
2.2: 12 h
2.3: 1.5 h
3.1: boron trifluoride diethyl etherate; triethylsilane / 8 h / 65 °C
4.1: potassium carbonate / acetonitrile; ethanol; water / 5 °C
4.2: 1 h
With
triethylsilane; aluminum (III) chloride; boron trifluoride diethyl etherate; tetrabutylammomium bromide; potassium carbonate;
In
ethanol; water; toluene; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; tetrabutylammomium bromide / toluene / 24 h / Reflux
1.2: 12 h
1.3: 1.5 h
2.1: boron trifluoride diethyl etherate; triethylsilane / 8 h / 65 °C
3.1: potassium carbonate / acetonitrile; ethanol; water / 5 °C
3.2: 1 h
With
triethylsilane; boron trifluoride diethyl etherate; tetrabutylammomium bromide; potassium carbonate;
In
ethanol; water; toluene; acetonitrile;