N'-{2-[4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]-acetyl}hydrazine carboxylic acid tert-butyl ester

Base Information

• Chemical Name: N'-{2-[4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]-acetyl}hydrazine carboxylic acid tert-butyl ester
• CAS No.: 1192235-22-5
• Molecular Formula: C₃₅H₃₆N₂O₇
• Molecular Weight: 596.68
• Mol file: 1192235-22-5.mol

Synonyms:N'-{2-[4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]-acetyl}hydrazine carboxylic acid tert-butyl ester

Chemical Property of N'-{2-[4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]-acetyl}hydrazine carboxylic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-{2-[4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]-acetyl}hydrazine carboxylic acid tert-butyl ester

There total 1 articles about N'-{2-[4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]-acetyl}hydrazine carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

t-butoxycarbonylhydrazine (870-46-2) + [4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]acetic acid (1192235-19-0) → N'-{2-[4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]-acetyl}hydrazine carboxylic acid tert-butyl ester (1192235-22-5)

Guidance literature:

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1016/j.bmc.2009.08.013

Reference yield: 82.0%

N'-{2-[4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]-acetyl}hydrazine carboxylic acid tert-butyl ester (1192235-22-5) → C35H34N2O6

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1016/j.bmc.2009.08.013

upstream raw materials:

t-butoxycarbonylhydrazine

[4,5-dibenzyloxy-2-(4-methoxybenzoyl)-phenyl]acetic acid