anhydro-7-p-chlorophenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxyde

Base Information

• Chemical Name: anhydro-7-p-chlorophenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxyde
• CAS No.: 107841-13-4
• Molecular Formula: C₁₁H₁₀ClN₅S₂
• Molecular Weight: 311.819

Synonyms:anhydro-7-p-chlorophenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxyde

Chemical Property of anhydro-7-p-chlorophenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxyde

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Technology Process of anhydro-7-p-chlorophenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxyde

There total 1 articles about anhydro-7-p-chlorophenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

4-Chlorophenyl isothiocyanate (2131-55-7) + 4-Amino-1-methyl-bis-1,2,4-triazolium iodide (86663-28-7) → anhydro-7-p-chlorophenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxyde (107841-13-4)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 6h; Ambient temperature; Irradiation; ultrasound;

DOI:10.1016/S0040-4020(01)87630-4

Reference yield: 80.0%

anhydro-7-p-chlorophenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxyde (107841-13-4) + methyl iodide (74-88-4) → 7-p-chlorophenyl-1-methyl-3,6-bis(methylthio)1.2.4-triazolo<4,3-b>-1,2,4-triazolium iodide

Guidance literature:

In benzene; for 24h; Ambient temperature;

DOI:10.1016/S0040-4020(01)87630-4

Reference yield: 78.0%

anhydro-7-p-chlorophenyl-1-methyl-3-methylthio-6-mercapto-1,2,4-triazolo<4,3-b>-1,2,4-triazole hydroxyde (107841-13-4) → (4-Chloro-phenyl)-(2-methyl-5-methylsulfanyl-2H-[1,2,4]triazol-3-yl)-cyanamide (107841-17-8)

Guidance literature:

In benzene; for 3h; Heating;

DOI:10.1016/S0040-4020(01)87630-4

upstream raw materials:

4-Chlorophenyl isothiocyanate

4-Amino-1-methyl-bis-1,2,4-triazolium iodide

Downstream raw materials:

(4-Chloro-phenyl)-(2-methyl-5-methylsulfanyl-2H-[1,2,4]triazol-3-yl)-cyanamide

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