2,6-dimethylphenyl (2R,3R,4S,5R,6R)-6-((1S,3S,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-3,5-dihydroxy-2,4-dimethylheptanoate

Base Information

• Chemical Name: 2,6-dimethylphenyl (2R,3R,4S,5R,6R)-6-((1S,3S,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-3,5-dihydroxy-2,4-dimethylheptanoate
• CAS No.: 1197360-43-2
• Molecular Formula: C₂₅H₃₈O₆
• Molecular Weight: 434.573

Synonyms:2,6-dimethylphenyl (2R,3R,4S,5R,6R)-6-((1S,3S,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-3,5-dihydroxy-2,4-dimethylheptanoate

Chemical Property of 2,6-dimethylphenyl (2R,3R,4S,5R,6R)-6-((1S,3S,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-3,5-dihydroxy-2,4-dimethylheptanoate

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Technology Process of 2,6-dimethylphenyl (2R,3R,4S,5R,6R)-6-((1S,3S,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-3,5-dihydroxy-2,4-dimethylheptanoate

There total 1 articles about 2,6-dimethylphenyl (2R,3R,4S,5R,6R)-6-((1S,3S,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-3,5-dihydroxy-2,4-dimethylheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2,6-dimethylphenyl (2R,3R,4R,5R,6R)-5-(benzyloxy)-6-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxabicyclo[3.2.1]octan-3-yl)-3-hydroxy-2,4-dimethylheptanoate (1197360-41-0) → 2,6-dimethylphenyl (2R,3R,4S,5R,6R)-6-((1S,3S,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-3,5-dihydroxy-2,4-dimethylheptanoate (1197360-43-2)

Guidance literature:

With 10% palladium on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 12h;

DOI:10.1021/jo901913h

Reference yield: 96.0%

2,6-dimethylphenyl (2R,3R,4S,5R,6R)-6-((1S,3S,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-3,5-dihydroxy-2,4-dimethylheptanoate (1197360-43-2) + 2,2-dimethoxy-propane (77-76-9) → 2,6-dimethylphenyl (R)-2-((4R,5S,6S)-6-((R)-1-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxabicyclo[3.2.1]octan-3-yl)ethyl)-2,2,5-trimethyl-1,3-dioxan-4-yl)propanoate (1197360-44-3)

Guidance literature:

With toluene-4-sulfonic acid; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jo901913h

upstream raw materials:

2,6-dimethylphenyl (2R,3R,4R,5R,6R)-5-(benzyloxy)-6-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxabicyclo[3.2.1]octan-3-yl)-3-hydroxy-2,4-dimethylheptanoate

Downstream raw materials:

2,6-dimethylphenyl (R)-2-((4R,5S,6S)-6-((R)-1-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxabicyclo[3.2.1]octan-3-yl)ethyl)-2,2,5-trimethyl-1,3-dioxan-4-yl)propanoate

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