1,3-Dioxane-4-aceticacid,6-(cyanomethyl)-2,2-dimethyl-,methylester(9CI)

Base Information

Chemical Name:1,3-Dioxane-4-aceticacid,6-(cyanomethyl)-2,2-dimethyl-,methylester(9CI)
CAS No.:791115-50-9
Molecular Formula:C₁₁H₁₇NO₄
Molecular Weight:227.26
Hs Code.:
Mol file:791115-50-9.mol

Synonyms:[6-(Cyanomethyl)-2,2-dimethyl-1,3-dioxan-4-yl]aceticacid methyl ester

Suppliers and Price of 1,3-Dioxane-4-aceticacid,6-(cyanomethyl)-2,2-dimethyl-,methylester(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dioxane-4-aceticacid,6-(cyanomethyl)-2,2-dimethyl-,methylester(9CI)

Chemical Property:

Boiling Point:331.1±17.0 °C(Predicted)
Density:1.054±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Technology Process of 1,3-Dioxane-4-aceticacid,6-(cyanomethyl)-2,2-dimethyl-,methylester(9CI)

There total 19 articles about 1,3-Dioxane-4-aceticacid,6-(cyanomethyl)-2,2-dimethyl-,methylester(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 773837-37-9
sodium cyanide

: 391218-16-9
2-((4R,6S)-6-(chloromethyl)-2,2-dimethyl-1,3-dioxan-4-yl)acetic acid methyl ester

: 791115-50-9
methyl 2-((4R,6R)-6-(cyanomethyl)-2,2-dimethyl-1,3-dioxan-4-yl)acetate

Guidance literature:: With copper(l) chloride; In dimethyl sulfoxide; at 120 - 130 ℃; for 24h;

Reference yield: 78.5%

: 791115-50-9
methyl 2-((4R,6R)-6-(cyanomethyl)-2,2-dimethyl-1,3-dioxan-4-yl)acetate

Guidance literature:: With boron trifluoride diethyl etherate; In tetrahydrofuran; at 60 ℃; for 6h; Inert atmosphere;

With benzenesulfonic acid; In water; toluene; at 35 ℃; for 4h;

at 40 ℃; for 4h;