tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}butanoyl)cyclopropanecarboxylate

Base Information

Chemical Name:tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}butanoyl)cyclopropanecarboxylate
CAS No.:1114546-97-2
Molecular Formula:C₂₀H₂₇NO₅
Molecular Weight:361.438
Hs Code.:

Synonyms:tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}butanoyl)cyclopropanecarboxylate

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Chemical Property of tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}butanoyl)cyclopropanecarboxylate

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Technology Process of tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}butanoyl)cyclopropanecarboxylate

There total 1 articles about tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}butanoyl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1114546-96-1
benzyl (4S)-4-ethyl-2,5-dioxo-1,3-oxazolidine-3-carboxylate

: 87661-20-9
tert-butyl cyclopropanecarboxylate

: 1114546-97-2
tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}butanoyl)cyclopropanecarboxylate

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

tert-butyl cyclopropanecarboxylate; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

benzyl (4S)-4-ethyl-2,5-dioxo-1,3-oxazolidine-3-carboxylate; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

Reference yield: 78.0%

: 1114546-97-2
tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}butanoyl)cyclopropanecarboxylate

: 1114546-99-4
tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}-1-hydroxybutyl)cyclopropanecarboxylate

Guidance literature:: tert-butyl 1-((2S)-2-{[(benzyloxy)carbonyl]amino}butanoyl)cyclopropanecarboxylate; With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h;

With water; ammonium chloride; In methanol;