7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene

Base Information

Chemical Name:7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene
CAS No.:1246672-15-0
Molecular Formula:C₁₄H₁₃N₅S
Molecular Weight:283.357
Hs Code.:

Synonyms:7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene

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Chemical Property of 7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene

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Technology Process of 7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene

There total 7 articles about 7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1246672-14-9
7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene-3-carboxylic acid

: 1246672-15-0
7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene

Guidance literature:: 7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene-3-carboxylic acid; With hydrogenchloride; In 1,4-dioxane; for 16h; Reflux;

With sodium hydrogencarbonate; In water;

Reference yield:

: 6299-25-8
4,6-Dichloro-2-(methylthio)pyrimidine

: 1246672-15-0
7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -78 °C

1.2: 4 h / -78 °C

2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 7 h / 100 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / Cooling with ice

4.1: hydrazine hydrate; triethylamine / 1,4-dioxane / 5 - 6 h / 20 °C

5.1: water; sodium hydroxide / ethanol / 3 h / 60 °C

6.1: hydrogenchloride / 1,4-dioxane / 16 h / Reflux

With hydrogenchloride; water; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 959070-42-9
4,6-dichloro-2-(methylthio)pyrimidine-5-carboxylic acid ethyl ester

: 1246672-15-0
7-(methylthio)-5-phenyl-1,3,4,5-tetrahydro-1,2,5,6,8-pentaazaacenaphthylene

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 7 h / 100 °C

2: lithium diisopropyl amide / tetrahydrofuran / Cooling with ice

3: hydrazine hydrate; triethylamine / 1,4-dioxane / 5 - 6 h / 20 °C

4: water; sodium hydroxide / ethanol / 3 h / 60 °C

5: hydrogenchloride / 1,4-dioxane / 16 h / Reflux

With hydrogenchloride; water; hydrazine hydrate; triethylamine; N-ethyl-N,N-diisopropylamine; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; ethanol; N,N-dimethyl-formamide;