C₂₇H₂₉N₇O₂S*C₂HF₃O₂

Base Information

Chemical Name:C₂₇H₂₉N₇O₂S*C₂HF₃O₂
CAS No.:1439400-73-3
Molecular Formula:C₂HF₃O₂*C₂₇H₂₉N₇O₂S
Molecular Weight:629.663
Hs Code.:

C<sub>27</sub>H<sub>29</sub>N<sub>7</sub>O<sub>2</sub>S*C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>

Synonyms:C₂₇H₂₉N₇O₂S*C₂HF₃O₂

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Chemical Property of C₂₇H₂₉N₇O₂S*C₂HF₃O₂

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Technology Process of C₂₇H₂₉N₇O₂S*C₂HF₃O₂

There total 8 articles about C₂₇H₂₉N₇O₂S*C₂HF₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1439394-27-0
C₃₂H₃₇N₇O₄S

: 76-05-1
trifluoroacetic acid

: 1439400-73-3
C₂₇H₂₉N₇O₂S*C₂HF₃O₂

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 0.333333h;

Reference yield:

: 103-80-0
phenylacetyl chloride

: 1439400-73-3
C₂₇H₂₉N₇O₂S*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: 1-methyl-pyrrolidin-2-one / 1.58 h / 19 - 28 °C

2: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 4 h / 19 °C / Inert atmosphere

3: trifluoroacetic acid / 2 h / 65 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C / Inert atmosphere

5: dichloromethane / 0.33 h / 0 - 20 °C

With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1439400-51-7
N-(6-iodopyridazin-3-yl)-2-phenylacetamide

: 1439400-73-3
C₂₇H₂₉N₇O₂S*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 5 steps

1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 60 °C / Inert atmosphere

2: hydrogen; 10 wt% Pd(OH)2 on carbon / ethanol; ethyl acetate / 1 h

3: trifluoroacetic acid / 2 h / 65 °C

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1.5 h / 0 - 20 °C / Inert atmosphere

5: dichloromethane / 0.33 h / 0 - 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 10 wt% Pd(OH)2 on carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;