1-(5'-p-tosyl-all-trans-decaprenyl)-2-methyl-3,4,5,6-tetramethoxybenzene

Base Information

Chemical Name:1-(5'-p-tosyl-all-trans-decaprenyl)-2-methyl-3,4,5,6-tetramethoxybenzene
CAS No.:94828-16-7
Molecular Formula:C₆₈H₁₀₂O₆S
Molecular Weight:1047.62
Hs Code.:

Synonyms:1-(5'-p-tosyl-all-trans-decaprenyl)-2-methyl-3,4,5,6-tetramethoxybenzene

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Chemical Property of 1-(5'-p-tosyl-all-trans-decaprenyl)-2-methyl-3,4,5,6-tetramethoxybenzene

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Technology Process of 1-(5'-p-tosyl-all-trans-decaprenyl)-2-methyl-3,4,5,6-tetramethoxybenzene

There total 4 articles about 1-(5'-p-tosyl-all-trans-decaprenyl)-2-methyl-3,4,5,6-tetramethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 70854-64-7
solanesyl p-tolyl sulphone

: 94828-11-2
1-((E)-4-Bromo-3-methyl-but-2-enyl)-2,3,4,5-tetramethoxy-6-methyl-benzene

: 94828-16-7
1-(5'-p-tosyl-all-trans-decaprenyl)-2-methyl-3,4,5,6-tetramethoxybenzene

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; hexane; at -70 - 0 ℃; for 2h;

Reference yield:

: 13190-97-1,540-03-4
solanesol

: 94828-16-7
1-(5'-p-tosyl-all-trans-decaprenyl)-2-methyl-3,4,5,6-tetramethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: PBr₃

2: 71 percent / Ambient temperature

3: 86 percent / 1.) hexamethylphosphoric triamide, BuLi / tetrahydrofuran; hexane / 2 h / -70 - 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; phosphorus tribromide; In tetrahydrofuran; hexane;

Reference yield:

: 52610-77-2
solanesyl bromide

: 94828-16-7
1-(5'-p-tosyl-all-trans-decaprenyl)-2-methyl-3,4,5,6-tetramethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Ambient temperature

2: 86 percent / 1.) hexamethylphosphoric triamide, BuLi / tetrahydrofuran; hexane / 2 h / -70 - 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; hexane;