2,2,2-trifluoro-1-(3-phenylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethan-1-one

Base Information

Chemical Name:2,2,2-trifluoro-1-(3-phenylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethan-1-one
CAS No.:182947-20-2
Molecular Formula:C₁₅H₁₁F₃O
Molecular Weight:264.247
Hs Code.:

Synonyms:2,2,2-trifluoro-1-(3-phenylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethan-1-one

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Chemical Property of 2,2,2-trifluoro-1-(3-phenylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethan-1-one

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Technology Process of 2,2,2-trifluoro-1-(3-phenylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethan-1-one

There total 5 articles about 2,2,2-trifluoro-1-(3-phenylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 58518-08-4
1,1,1-trifluoro-4-phenylbut-3-yn-2-one

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 182947-20-2
2,2,2-trifluoro-1-(3-phenylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethan-1-one

Guidance literature:: at 45 - 50 ℃; for 8h;

Reference yield: 86.0%

: 1229115-79-0
2,2,2-trifluoro-1-(3-pyrrolidin-1-ylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethanone

: 100-58-3
phenylmagnesium bromide

: 182947-20-2
2,2,2-trifluoro-1-(3-phenylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethan-1-one

Guidance literature:: 2,2,2-trifluoro-1-(3-pyrrolidin-1-ylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethanone; phenylmagnesium bromide; at 20 ℃; Inert atmosphere;

With sodium dihydrogenphosphate; water; regioselective reaction;
DOI:10.1016/j.tet.2010.03.026

Reference yield:

: C₁₇H₁₇F₃N⁽¹⁺⁾*CF₃O₃S^(1-)

: 182947-20-2
2,2,2-trifluoro-1-(3-phenylbicyclo[2.2.1]hepta-2,5-dien-2-yl)ethan-1-one

Guidance literature:: With water; potassium carbonate; In acetonitrile; at 20 ℃; for 0.166667h; Inert atmosphere; Schlenk technique;
DOI:10.3762/BJOC.16.173