2,2-dihydro 2-methyl 2,2-diphenyl 3,4-methano 1,2-oxaphospholanne

Base Information

• Chemical Name: 2,2-dihydro 2-methyl 2,2-diphenyl 3,4-methano 1,2-oxaphospholanne
• CAS No.: 106938-52-7
• Molecular Formula: C₁₇H₁₉OP
• Molecular Weight: 270.311
• Mol file: 106938-52-7.mol

Synonyms:2,2-dihydro 2-methyl 2,2-diphenyl 3,4-methano 1,2-oxaphospholanne

Chemical Property of 2,2-dihydro 2-methyl 2,2-diphenyl 3,4-methano 1,2-oxaphospholanne

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,2-dihydro 2-methyl 2,2-diphenyl 3,4-methano 1,2-oxaphospholanne

There total 1 articles about 2,2-dihydro 2-methyl 2,2-diphenyl 3,4-methano 1,2-oxaphospholanne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-bromoethyl)oxirane (13287-42-8) + diphenyl(methyl)phosphine (1486-28-8) → 2,2-dihydro 2-methyl 2,2-diphenyl 3,4-methano 1,2-oxaphospholanne (106938-52-7)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1016/S0040-4039(00)84408-1

Reference yield: 86.0%

benzophenone (119-61-9) + 2,2-dihydro 2-methyl 2,2-diphenyl 3,4-methano 1,2-oxaphospholanne (106938-52-7) → 1,1-Diphenylethylene (530-48-3) + [2-(Diphenyl-phosphinoyl)-cyclopropyl]-methanol (60329-16-0)

Guidance literature:

for 5h;

DOI:10.1016/S0040-4039(00)84408-1

Reference yield: 78.0%

para-chloroacetophenone (99-91-2) + 2,2-dihydro 2-methyl 2,2-diphenyl 3,4-methano 1,2-oxaphospholanne (106938-52-7) → 1-chloro-4-(1-methylethenyl)-benzene (1712-70-5) + [2-(Diphenyl-phosphinoyl)-cyclopropyl]-methanol (60329-16-0)

Guidance literature:

for 5h;

DOI:10.1016/S0040-4039(00)84408-1

upstream raw materials:

(2-bromoethyl)oxirane

diphenyl(methyl)phosphine

Downstream raw materials:

1,1-Diphenylethylene

[2-(Diphenyl-phosphinoyl)-cyclopropyl]-methanol

1-undecene

1-chloro-4-(1-methylethenyl)-benzene