methyl 10-phenyl-3,6,9-trioxadecanoate

Base Information

Chemical Name:methyl 10-phenyl-3,6,9-trioxadecanoate
CAS No.:86520-56-1
Molecular Formula:C₁₄H₂₀O₅
Molecular Weight:268.31
Hs Code.:

Synonyms:methyl 10-phenyl-3,6,9-trioxadecanoate

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Chemical Property of methyl 10-phenyl-3,6,9-trioxadecanoate

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Technology Process of methyl 10-phenyl-3,6,9-trioxadecanoate

There total 2 articles about methyl 10-phenyl-3,6,9-trioxadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 2050-25-1,1201808-31-2
diethylene glycol monobenzyl ether

: 96-32-2
bromoacetic acid methyl ester

: 86520-56-1
methyl 10-phenyl-3,6,9-trioxadecanoate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 4h;
DOI:10.1016/0008-6215(86)80016-7

Reference yield:

: 100-44-7
benzyl chloride

: 86520-56-1
methyl 10-phenyl-3,6,9-trioxadecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / KOH / dioxane / 2 h / 80 °C

2: 66 percent / NaH / tetrahydrofuran / 4 h / 0 °C

With potassium hydroxide; sodium hydride; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/0008-6215(86)80016-7

Reference yield:

: 86520-56-1
methyl 10-phenyl-3,6,9-trioxadecanoate

: 106294-95-5
7-methoxycarbonyl-3,6-dioxaheptyl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / H₂ / 10percent Pd/C / methanol / 18 h

2: 67.8 percent / calcium sulfate, mercuric cyanide / CH₂Cl₂ / 30 h / Ambient temperature

3: 86.5 percent / NaOMe / methanol / 2 h / Ambient temperature

4: 84 percent / p-toluenesulfonic acid monohydrate / 1 h / 65 - 100 °C

With calcium sulfate; hydrogen; sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/0008-6215(86)80016-7