C₅₀H₄₈BrClF₂O₅

Base Information

Chemical Name:C₅₀H₄₈BrClF₂O₅
CAS No.:1413374-37-4
Molecular Formula:C₅₀H₄₈BrClF₂O₅
Molecular Weight:882.282
Hs Code.:

C<sub>50</sub>H<sub>48</sub>BrClF<sub>2</sub>O<sub>5</sub>

Synonyms:C₅₀H₄₈BrClF₂O₅

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Chemical Property of C₅₀H₄₈BrClF₂O₅

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Technology Process of C₅₀H₄₈BrClF₂O₅

There total 20 articles about C₅₀H₄₈BrClF₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: C₅₀H₄₉ClF₂O₆

: 1413374-37-4
C₅₀H₄₈BrClF₂O₅

Guidance literature:: C₅₀H₄₉ClF₂O₆; With dibromo sulfoxide; In dichloromethane; at -40 - 0 ℃; for 5h; Inert atmosphere;

With pyridine; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 110391-10-1
(4R,5S,6R)-4,5,6-tris(benzyloxy)-3-((benzyloxy)methyl)-2-cyclohexen-1-one

: 1413374-37-4
C₅₀H₄₈BrClF₂O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

1.2: 0.75 h

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2.2: 12 h / 40 °C

3.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 0 - 20 °C

4.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

5.1: hydrogenchloride; methanol / dichloromethane / 20 °C

6.1: pyridine / dmap / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

7.1: diethylamino-sulfur trifluoride / dichloromethane / 16 h / 20 °C / Inert atmosphere

8.1: sodium methylate; methanol / 20 °C / Industry scale

9.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

9.2: 2 h / 20 °C

10.1: dibromo sulfoxide / dichloromethane / 5 h / -40 - 0 °C / Inert atmosphere

10.2: 1 h / 0 °C

With pyridine; 1H-imidazole; hydrogenchloride; methanol; dibromo sulfoxide; diethylamino-sulfur trifluoride; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; sodium methylate; Dess-Martin periodane; dmap; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 99695-34-8
(1R,2S,3S,4R)-2,3,4-tri-O-benzyl-5-(benzyloxymethyl)-cyclohex-5-ene-1,2,3,4-tetrol

: 1413374-37-4
C₅₀H₄₈BrClF₂O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: phosphorus pentoxide / chloroform / 1 h / 20 °C / Inert atmosphere

2.1: sodium methylate; methanol / 20 °C / Industry scale

3.1: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

3.2: 2 h / 20 °C

4.1: dibromo sulfoxide / dichloromethane / 5 h / -40 - 0 °C / Inert atmosphere

4.2: 1 h / 0 °C

With methanol; dibromo sulfoxide; phosphorus pentoxide; sodium methylate; Dess-Martin periodane; In dichloromethane; chloroform;