C₄₅H₅₃NO₁₃

Base Information

• Chemical Name: C₄₅H₅₃NO₁₃
• CAS No.: 1440522-39-3
• Molecular Formula: C₄₅H₅₃NO₁₃
• Molecular Weight: 815.915
• Mol file: 1440522-39-3.mol

Synonyms:C₄₅H₅₃NO₁₃

Chemical Property of C₄₅H₅₃NO₁₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₅H₅₃NO₁₃

There total 9 articles about C₄₅H₅₃NO₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

C49H61NO14 → C45H53NO13 (1440522-39-3)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 0 - 20 ℃; for 4h; Inert atmosphere;

DOI:10.1021/jm400479p

Reference yield: 25.0%

C51H65NO16 → C45H53NO13 (1440522-39-3) + C47H57NO15 (1440522-41-7)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 0 - 20 ℃; for 4h; Inert atmosphere;

DOI:10.1021/jm400479p

Reference yield:

C39H54O11Si (1035113-20-2) → C45H53NO13 (1440522-39-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: hydrogenchloride / water; tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; In tetrahydrofuran; water;

DOI:10.1021/jm400479p

upstream raw materials:

C₃₃H₄₀O₁₁

1-tert-butoxycarbonyl-(3R,4S)-3-EEO-4-phenylazetidin-2-one

acetoxybrevifoliol

C₃₉H₅₄O₁₁Si

Refernces