N-(diphenyl)acetyl-4-[(2-methoxy-4-methoxycarbonyl)benzylidene]piperidine

Base Information

Chemical Name:N-(diphenyl)acetyl-4-[(2-methoxy-4-methoxycarbonyl)benzylidene]piperidine
CAS No.:455323-48-5
Molecular Formula:C₂₉H₂₉NO₄
Molecular Weight:455.554
Hs Code.:

Synonyms:N-(diphenyl)acetyl-4-[(2-methoxy-4-methoxycarbonyl)benzylidene]piperidine

Suppliers and Price of N-(diphenyl)acetyl-4-[(2-methoxy-4-methoxycarbonyl)benzylidene]piperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(diphenyl)acetyl-4-[(2-methoxy-4-methoxycarbonyl)benzylidene]piperidine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of N-(diphenyl)acetyl-4-[(2-methoxy-4-methoxycarbonyl)benzylidene]piperidine

There total 2 articles about N-(diphenyl)acetyl-4-[(2-methoxy-4-methoxycarbonyl)benzylidene]piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 161491-32-3
N-(diphenyl)acetyl-4-piperidone

: 2-methoxy-4-methoxycarbonylbenzyltriphenylphosphonium bromide

: 455323-48-5
N-(diphenyl)acetyl-4-[(2-methoxy-4-methoxycarbonyl)benzylidene]piperidine

Guidance literature:: 2-methoxy-4-methoxycarbonylbenzyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

N-(diphenyl)acetyl-4-piperidone; In tetrahydrofuran; hexane; at 20 ℃; Further stages.;
DOI:10.1021/jm0208471

Reference yield:

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 455323-48-5
N-(diphenyl)acetyl-4-[(2-methoxy-4-methoxycarbonyl)benzylidene]piperidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 62 percent / toluene / 5 h / 120 °C

2.1: n-BuLi / hexane; tetrahydrofuran / -78 °C

2.2: 10 percent / tetrahydrofuran; hexane / 20 °C

With n-butyllithium; In tetrahydrofuran; hexane; toluene; 2.2: Wittig olefination;
DOI:10.1021/jm0208471