Bicyclo[6.1.0]non-2-ene-9-carbonyl chloride, (1alpha,8alpha,9alpha)- (9CI)

Base Information

• Chemical Name: Bicyclo[6.1.0]non-2-ene-9-carbonyl chloride, (1alpha,8alpha,9alpha)- (9CI)
• CAS No.: 79549-91-0
• Molecular Formula: C₁₀H₁₃ClO
• Molecular Weight: 184.666
• Mol file: 79549-91-0.mol

Synonyms:Bicyclo[6.1.0]non-2-ene-9-carbonyl chloride, (1alpha,8alpha,9alpha)- (9CI)

Chemical Property of Bicyclo[6.1.0]non-2-ene-9-carbonyl chloride, (1alpha,8alpha,9alpha)- (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bicyclo[6.1.0]non-2-ene-9-carbonyl chloride, (1alpha,8alpha,9alpha)- (9CI)

There total 4 articles about Bicyclo[6.1.0]non-2-ene-9-carbonyl chloride, (1alpha,8alpha,9alpha)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(Z)-Bicyclo[6.1.0]non-2-ene-9-carboxylic acid (28860-80-2) → (Z)-Bicyclo[6.1.0]non-2-ene-9-carbonyl chloride (28860-76-6,79549-91-0)

Guidance literature:

With thionyl chloride; for 3h;

Reference yield:

(Z)-Bicyclo[6.1.0]non-2-ene-9-carboxylic acid (28860-80-2) → (Z)-Bicyclo[6.1.0]non-2-ene-9-carbonyl chloride (28860-76-6,79549-91-0)

Guidance literature:

With thionyl chloride;

DOI:10.1021/ja00713a033

Reference yield:

1,3-cyclooctadiene (186983-16-4) → (Z)-Bicyclo[6.1.0]non-2-ene-9-carbonyl chloride (28860-76-6,79549-91-0)

Guidance literature:

Multi-step reaction with 3 steps

1: CuSO₄

2: aq. NaOH

3: SOCl₂

With sodium hydroxide; thionyl chloride; copper(II) sulfate;

DOI:10.1021/ja00713a033

upstream raw materials:

(Z)-Bicyclo[6.1.0]non-2-ene-9-carboxylic acid

(Z)-Bicyclo[6.1.0]non-2-ene-9-carboxylic acid

1,3-cyclooctadiene

(Z)-Bicyclo[6.1.0]non-2-ene-9-carboxylic acid ethyl ester