(3S,4R)-6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid tert-butyl ester

Base Information

Chemical Name:(3S,4R)-6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid tert-butyl ester
CAS No.:223437-58-9
Molecular Formula:C₃₈H₅₁NO₅Si₂
Molecular Weight:657.998
Hs Code.:

Synonyms:(3S,4R)-6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid tert-butyl ester

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Chemical Property of (3S,4R)-6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid tert-butyl ester

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Technology Process of (3S,4R)-6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid tert-butyl ester

There total 4 articles about (3S,4R)-6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 159276-68-3
(4S,5R)-4,5-Bis-(dimethyl-p-tolyl-silanyl)-oxepane-2,7-dione

: 223437-58-9
(3S,4R)-6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: BuLi / tetrahydrofuran; hexane / 1.) -40 deg C, 2.) -78 deg C to r.t., 3 h

2: (COCl)2 / dimethylformamide / 2 h / Ambient temperature

3: DMAP / Ambient temperature

With dmap; n-butyllithium; oxalyl dichloride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1039/a808838a

Reference yield:

: 215110-55-7
(3R,4S)-3,4-Bis-(dimethyl-p-tolyl-silanyl)-hexanedioic acid

: 223437-58-9
(3S,4R)-6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / DCCI / CH₂Cl₂ / 12 h / Ambient temperature

2: BuLi / tetrahydrofuran; hexane / 1.) -40 deg C, 2.) -78 deg C to r.t., 3 h

3: (COCl)2 / dimethylformamide / 2 h / Ambient temperature

4: DMAP / Ambient temperature

With dmap; n-butyllithium; oxalyl dichloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/a808838a

Reference yield:

: 6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid

: 223437-58-9
(3S,4R)-6-((S)-4-Benzyl-2-oxo-oxazolidin-3-yl)-3,4-bis-(dimethyl-p-tolyl-silanyl)-6-oxo-hexanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: (COCl)2 / dimethylformamide / 2 h / Ambient temperature

2: DMAP / Ambient temperature

With dmap; oxalyl dichloride; In N,N-dimethyl-formamide;
DOI:10.1039/a808838a