N-(4-((2-(adamantan-1-yl)ethyl)amino)-3-fluorophenyl)-3-oxobutan amide

Base Information

Chemical Name:N-(4-((2-(adamantan-1-yl)ethyl)amino)-3-fluorophenyl)-3-oxobutan amide
CAS No.:1542259-35-7
Molecular Formula:C₂₂H₂₉FN₂O₂
Molecular Weight:372.483
Hs Code.:

Synonyms:N-(4-((2-(adamantan-1-yl)ethyl)amino)-3-fluorophenyl)-3-oxobutan amide

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Chemical Property of N-(4-((2-(adamantan-1-yl)ethyl)amino)-3-fluorophenyl)-3-oxobutan amide

Chemical Property:

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Technology Process of N-(4-((2-(adamantan-1-yl)ethyl)amino)-3-fluorophenyl)-3-oxobutan amide

There total 4 articles about N-(4-((2-(adamantan-1-yl)ethyl)amino)-3-fluorophenyl)-3-oxobutan amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 691-45-2
acetylketene

: 1542259-34-6
N¹-(2-(adamantan-1-yl)ethyl)-2-fluorobenzene-1,4-diamine

: 1542259-35-7
N-(4-((2-(adamantan-1-yl)ethyl)amino)-3-fluorophenyl)-3-oxobutan amide

Guidance literature:: In ethyl acetate; at 90 ℃;

Reference yield:

: 369-35-7
2-fluoro-4-nitroaniline

: 1542259-35-7
N-(4-((2-(adamantan-1-yl)ethyl)amino)-3-fluorophenyl)-3-oxobutan amide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 140 °C

2: hydrogenchloride; iron / methanol; water / 0.5 h / 65 °C

3: ethyl acetate / 90 °C

With hydrogenchloride; iron; potassium carbonate; potassium iodide; In methanol; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 1542259-33-5
N-(2-(adamantan-1-yl)ethyl)-2-fluoro-4-nitroaniline

: 1542259-35-7
N-(4-((2-(adamantan-1-yl)ethyl)amino)-3-fluorophenyl)-3-oxobutan amide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; iron / methanol; water / 0.5 h / 65 °C

2: ethyl acetate / 90 °C

With hydrogenchloride; iron; In methanol; water; ethyl acetate;