S-(2-chloro-3-fluoro-6-nitrophenyl)-α-mercapto-4-fluorobenzeneacetic acid

Base Information

Chemical Name:S-(2-chloro-3-fluoro-6-nitrophenyl)-α-mercapto-4-fluorobenzeneacetic acid
CAS No.:151295-13-5
Molecular Formula:C₁₄H₈ClF₂NO₄S
Molecular Weight:359.738
Hs Code.:

Synonyms:S-(2-chloro-3-fluoro-6-nitrophenyl)-α-mercapto-4-fluorobenzeneacetic acid

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Chemical Property of S-(2-chloro-3-fluoro-6-nitrophenyl)-α-mercapto-4-fluorobenzeneacetic acid

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Technology Process of S-(2-chloro-3-fluoro-6-nitrophenyl)-α-mercapto-4-fluorobenzeneacetic acid

There total 2 articles about S-(2-chloro-3-fluoro-6-nitrophenyl)-α-mercapto-4-fluorobenzeneacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 29270-33-5
2-bromo-2-(4-fluorophenyl)acetic acid

: 2-chloro-3-fluoro-6-nitrobenzene-1-thiol

: 151295-13-5
S-(2-chloro-3-fluoro-6-nitrophenyl)-α-mercapto-4-fluorobenzeneacetic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; for 2h; Heating;
DOI:10.1021/jm00074a028

Reference yield:

: 405-50-5
p-Fluorophenylacetic acid

: 151295-13-5
S-(2-chloro-3-fluoro-6-nitrophenyl)-α-mercapto-4-fluorobenzeneacetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Br₂ / CCl₄ / 2 h / Heating; Irradiation

2: 77 percent / 1.) NaOH / H₂O; ethanol / 2 h / Heating

With sodium hydroxide; bromine; In tetrachloromethane; ethanol; water;
DOI:10.1021/jm00074a028