ethyl 2-(((6-(trans-4-tert-butylcyclohexyloxy)naphthalen-2-yl)methyl)(methyl)amino)acetate

Base Information

Chemical Name:ethyl 2-(((6-(trans-4-tert-butylcyclohexyloxy)naphthalen-2-yl)methyl)(methyl)amino)acetate
CAS No.:1266115-76-7
Molecular Formula:C₂₆H₃₇NO₃
Molecular Weight:411.585
Hs Code.:

Synonyms:ethyl 2-(((6-(trans-4-tert-butylcyclohexyloxy)naphthalen-2-yl)methyl)(methyl)amino)acetate

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Chemical Property of ethyl 2-(((6-(trans-4-tert-butylcyclohexyloxy)naphthalen-2-yl)methyl)(methyl)amino)acetate

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Technology Process of ethyl 2-(((6-(trans-4-tert-butylcyclohexyloxy)naphthalen-2-yl)methyl)(methyl)amino)acetate

There total 8 articles about ethyl 2-(((6-(trans-4-tert-butylcyclohexyloxy)naphthalen-2-yl)methyl)(methyl)amino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 13200-60-7
Sarcosine ethyl ester

: 1266115-60-9
6-(trans-4-tert-butylcyclohexyloxy)-2-naphthaldehyde

: 1266115-76-7
ethyl 2-(((6-(trans-4-tert-butylcyclohexyloxy)naphthalen-2-yl)methyl)(methyl)amino)acetate

Guidance literature:: Sarcosine ethyl ester; 6-(trans-4-tert-butylcyclohexyloxy)-2-naphthaldehyde; In ethanol; for 3h; Reflux;

With ethanol; sodium cyanoborohydride; at 23 ℃; for 1h; Reflux;

Reference yield:

: 15231-91-1
6-bromo-naphthalen-2-ol

: 1266115-76-7
ethyl 2-(((6-(trans-4-tert-butylcyclohexyloxy)naphthalen-2-yl)methyl)(methyl)amino)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: caesium carbonate / butanone; tert-butyl alcohol / 0.17 h / 110 °C

1.2: 15 h / 110 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C

2.3: pH 6

3.1: ethanol / 3 h / Reflux

3.2: 1 h / 23 °C / Reflux

With n-butyllithium; caesium carbonate; In tetrahydrofuran; ethanol; butanone; tert-butyl alcohol;

Reference yield:

: 17295-11-3
methyl 6-hydroxynaphthalene-2-carboxylate

: 1266115-76-7
ethyl 2-(((6-(trans-4-tert-butylcyclohexyloxy)naphthalen-2-yl)methyl)(methyl)amino)acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 6 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C

2.2: 1 h / 20 °C

3.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

4.1: ethanol / 3 h / Reflux

4.2: 1 h / 23 °C / Reflux

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; Dess-Martin periodane; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; toluene;