C₃₂H₃₁NO₄

Base Information

Chemical Name:C₃₂H₃₁NO₄
CAS No.:1221269-84-6
Molecular Formula:C₃₂H₃₁NO₄
Molecular Weight:493.602
Hs Code.:

C<sub>32</sub>H<sub>31</sub>NO<sub>4</sub>

Synonyms:C₃₂H₃₁NO₄

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Chemical Property of C₃₂H₃₁NO₄

Chemical Property:

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Technology Process of C₃₂H₃₁NO₄

There total 5 articles about C₃₂H₃₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1221269-81-3
C₃₁H₂₉NO₅

: 1221269-84-6
C₃₂H₃₁NO₄

Guidance literature:: With potassium tert-butylate; methyl-triphenylphosphonium iodide; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1039/b917065k

Reference yield:

: 90064-47-4
4-iodo-2,5-dimethoxybenzenecarbaldehyde

: 1221269-84-6
C₃₂H₃₁NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: copper(I) oxide / N,N-dimethyl acetamide / 72 h / 190 °C

2: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

3: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 2,6-di-tert-butyl-4-methyl-phenol; sodium carbonate / tetrahydrofuran / 24 h / 110 °C

4: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C

With copper(I) oxide; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 2,6-di-tert-butyl-4-methyl-phenol; potassium tert-butylate; methyl-triphenylphosphonium iodide; sodium carbonate; In tetrahydrofuran; N,N-dimethyl acetamide;
DOI:10.1039/b917065k

Reference yield:

: 93-02-7
2,5-dimethoxybenzaldehyde

: 1221269-84-6
C₃₂H₃₁NO₄

Guidance literature:: Multi-step reaction with 5 steps

1: iodine; silver nitrate / methanol / 7 h / 20 °C

2: copper(I) oxide / N,N-dimethyl acetamide / 72 h / 190 °C

3: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

4: trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 2,6-di-tert-butyl-4-methyl-phenol; sodium carbonate / tetrahydrofuran / 24 h / 110 °C

5: potassium tert-butylate; methyl-triphenylphosphonium iodide / tetrahydrofuran / 4 h / 20 °C

With copper(I) oxide; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 2,6-di-tert-butyl-4-methyl-phenol; potassium tert-butylate; iodine; methyl-triphenylphosphonium iodide; sodium carbonate; silver nitrate; In tetrahydrofuran; methanol; N,N-dimethyl acetamide;
DOI:10.1039/b917065k