(E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide

Base Information

Chemical Name:(E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide
CAS No.:220378-44-9
Molecular Formula:C₃₃H₂₈ClN₃O₂S
Molecular Weight:566.123
Hs Code.:

Synonyms:(E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide

Suppliers and Price of (E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide

There total 3 articles about (E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42060-30-0
N-(4-chloro-benzyl)-methanesulfonamide

: 220378-44-9
(E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 89 percent / N,N-4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h

2.1: LDA / tetrahydrofuran / 1 h / -78 °C

2.2: 11 percent / tetrahydrofuran / -78 - 20 °C

With dmap; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0968-0896(01)00295-4

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 220378-44-9
(E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 81 percent / Et₃N / CH₂Cl₂ / 2 h

2.1: 89 percent / N,N-4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h

3.1: LDA / tetrahydrofuran / 1 h / -78 °C

3.2: 11 percent / tetrahydrofuran / -78 - 20 °C

With dmap; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0968-0896(01)00295-4

Reference yield:

: 138408-37-4
1-(triphenylmethyl)-4-(3-hydroxyprop-1-enyl)imidazole

: 220378-44-9
(E,E)-4-(1-trityl-1H-imidazol-4-yl)buta-1,3-diene-1-sulfonic acid 4-chlorobenzylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 72 percent / manganese dioxide / CHCl₃ / 2.5 h / Heating

2.1: LDA / tetrahydrofuran / 1 h / -78 °C

2.2: 11 percent / tetrahydrofuran / -78 - 20 °C

With manganese(IV) oxide; lithium diisopropyl amide; In tetrahydrofuran; chloroform;
DOI:10.1016/S0968-0896(01)00295-4