(2S,4S,5R)-4-methyl-5-phenyl-2-(1-phenyl-vinyl)-3-(toluene-4'-sulfonyl)-oxazolidine

Base Information

Chemical Name:(2S,4S,5R)-4-methyl-5-phenyl-2-(1-phenyl-vinyl)-3-(toluene-4'-sulfonyl)-oxazolidine
CAS No.:166189-48-6
Molecular Formula:C₂₅H₂₅NO₃S
Molecular Weight:419.544
Hs Code.:

Synonyms:(2S,4S,5R)-4-methyl-5-phenyl-2-(1-phenyl-vinyl)-3-(toluene-4'-sulfonyl)-oxazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4S,5R)-4-methyl-5-phenyl-2-(1-phenyl-vinyl)-3-(toluene-4'-sulfonyl)-oxazolidine

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Technology Process of (2S,4S,5R)-4-methyl-5-phenyl-2-(1-phenyl-vinyl)-3-(toluene-4'-sulfonyl)-oxazolidine

There total 1 articles about (2S,4S,5R)-4-methyl-5-phenyl-2-(1-phenyl-vinyl)-3-(toluene-4'-sulfonyl)-oxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 108591-33-9
N-((1R,2S)-1-hydroxy-1-phenylpropan-2-yl)-4-methylbenzene sulfonamide

: 80234-04-4
2-phenylacrylaldehyde diethyl acetal

: 166189-48-6
(2S,4S,5R)-4-methyl-5-phenyl-2-(1-phenyl-vinyl)-3-(toluene-4'-sulfonyl)-oxazolidine

Guidance literature:: With pyridinium p-toluenesulfonate; In benzene; for 4h; Heating;
DOI:10.1016/S0040-4020(96)01087-3

Reference yield: 80.0%

: 166189-48-6
(2S,4S,5R)-4-methyl-5-phenyl-2-(1-phenyl-vinyl)-3-(toluene-4'-sulfonyl)-oxazolidine

: (2RS,2'S,4'S,5'R)-2-[4'-methyl-5'-phenyl-3'-(toluene-4''-sulfonyl)-oxazolidin-2'-yl]-1-phenyl-ethane-1,2-diol

Guidance literature:: With osmium (III) chloride; trimethylamine-N-oxide; In water; acetone; for 1h;
DOI:10.1016/S0040-4020(96)01087-3

Reference yield:

: 166189-48-6
(2S,4S,5R)-4-methyl-5-phenyl-2-(1-phenyl-vinyl)-3-(toluene-4'-sulfonyl)-oxazolidine

: (1R,2'S,4'S,5'R)-1-[4'-methyl-5'-phenyl-3'-(toluene-4''-sulfonyl)-oxazolidin-2'-yl]-1-phenyl-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / OsCl₃, Me₃NO*2H₂O / acetone; H₂O / 1 h

2: 40 percent / NaIO₄ / dioxane; H₂O / 1 h / Ambient temperature

3: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

With sodium periodate; osmium (III) chloride; trimethylamine-N-oxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; water; acetone;
DOI:10.1016/S0040-4020(96)01087-3