N-<β-(5'-Benzyloxy-3'-indolyl)-ethyl>-4-(1-hydroxymethyl-propyl)-pyridiniumbromid

Base Information

Chemical Name:N-<β-(5'-Benzyloxy-3'-indolyl)-ethyl>-4-(1-hydroxymethyl-propyl)-pyridiniumbromid
CAS No.:22311-12-2
Molecular Formula:Br*C₂₆H₂₉N₂O₂
Molecular Weight:481.432
Hs Code.:

Synonyms:N-<β-(5'-Benzyloxy-3'-indolyl)-ethyl>-4-(1-hydroxymethyl-propyl)-pyridiniumbromid

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Chemical Property of N-<β-(5'-Benzyloxy-3'-indolyl)-ethyl>-4-(1-hydroxymethyl-propyl)-pyridiniumbromid

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Technology Process of N-<β-(5'-Benzyloxy-3'-indolyl)-ethyl>-4-(1-hydroxymethyl-propyl)-pyridiniumbromid

There total 4 articles about N-<β-(5'-Benzyloxy-3'-indolyl)-ethyl>-4-(1-hydroxymethyl-propyl)-pyridiniumbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 132148-52-8
2-(4'-pyridyl)butanol

: 132148-51-7
5-(benzyloxy)-3-(2-bromoethyl)-1H-indole

: 22311-12-2
N-<β-(5'-Benzyloxy-3'-indolyl)-ethyl>-4-(1-hydroxymethyl-propyl)-pyridiniumbromid

Guidance literature:: DOI:10.1016/S0040-4020(01)90085-7

Reference yield:

: 4382-53-0
2-(5-benzyloxy-1H-indol-3-yl)acetic acid

: 22311-12-2
N-<β-(5'-Benzyloxy-3'-indolyl)-ethyl>-4-(1-hydroxymethyl-propyl)-pyridiniumbromid

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / LiAlH₄ / tetrahydrofuran / 3.5 h / Ambient temperature

2: 51 percent / diethyl ether / 1.) -5 deg C, 1.5 h 2.) refrigerator, overnight;

3: 96 percent

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(01)90085-7

Reference yield:

: 41339-61-1
5-benzyloxy-3-(2-hydroxyethyl)indole

: 22311-12-2
N-<β-(5'-Benzyloxy-3'-indolyl)-ethyl>-4-(1-hydroxymethyl-propyl)-pyridiniumbromid

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / diethyl ether / 1.) -5 deg C, 1.5 h 2.) refrigerator, overnight;

2: 96 percent

In diethyl ether;
DOI:10.1016/S0040-4020(01)90085-7