2-cyclohexylallyl ethyl carbonate

Base Information

Chemical Name:2-cyclohexylallyl ethyl carbonate
CAS No.:1415610-54-6
Molecular Formula:C₁₂H₂₀O₃
Molecular Weight:212.289
Hs Code.:

Synonyms:2-cyclohexylallyl ethyl carbonate

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Chemical Property of 2-cyclohexylallyl ethyl carbonate

Chemical Property:

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Technology Process of 2-cyclohexylallyl ethyl carbonate

There total 1 articles about 2-cyclohexylallyl ethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 7697-55-4
2-cyclohexylprop-2-en-1-ol

: 541-41-3
chloroformic acid ethyl ester

: 1415610-54-6
2-cyclohexylallyl ethyl carbonate

Guidance literature:: With pyridine; In tetrahydrofuran; at 0 ℃; for 3.16667h;
DOI:10.1039/c2cc36199j

Reference yield:

: 1415610-54-6
2-cyclohexylallyl ethyl carbonate

: 1415610-33-1
(S)-3-cyclohexyl-4-(4,4,6-trimethyl-1,3,2-dioxaborato)butanoic acid phenyl amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 16 h / 50 °C / 3620.13 Torr

2.1: water; sodium hydroxide / ethanol / 20 °C

3.1: dmap / dichloromethane / 5 h / 0 °C

3.2: 0 - 20 °C

4.1: bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2-(2,3,4,5-tetrahydrobenzo[b]oxepin-3-yl)acetic acid tert-butyl ester / tetrahydrofuran / 40 °C

With dmap; bis(norbornadiene)rhodium(l)tetrafluoroborate; (R)-2-(2,3,4,5-tetrahydrobenzo[b]oxepin-3-yl)acetic acid tert-butyl ester; water; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/c2cc36199j

Reference yield:

: 1415610-54-6
2-cyclohexylallyl ethyl carbonate

: 1415610-27-3
3-cyclohexyl-3-butenoic acid phenyl amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 16 h / 50 °C / 3620.13 Torr

2.1: water; sodium hydroxide / ethanol / 20 °C

3.1: dmap / dichloromethane / 5 h / 0 °C

3.2: 0 - 20 °C

With dmap; water; sodium hydroxide; In ethanol; dichloromethane;
DOI:10.1039/c2cc36199j