C₂₃H₃₁NO₅Si

Base Information

• Chemical Name: C₂₃H₃₁NO₅Si
• CAS No.: 1401229-70-6
• Molecular Formula: C₂₃H₃₁NO₅Si
• Molecular Weight: 429.588
• Mol file: 1401229-70-6.mol

Synonyms:C₂₃H₃₁NO₅Si

Chemical Property of C₂₃H₃₁NO₅Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₁NO₅Si

There total 2 articles about C₂₃H₃₁NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) → C23H31NO5Si (1401229-70-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / water; 1,4-dioxane / 23 h / 0 - 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 30 h / 0 - 20 °C

With 1H-imidazole; sodium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;

DOI:10.1021/ol3024506

Reference yield:

tyrosine (556-02-5,18875-48-4,25619-78-7,30704-25-7) → C23H31NO5Si (1401229-70-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / water; 1,4-dioxane / 23 h / 0 - 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 30 h / 0 - 20 °C

With 1H-imidazole; sodium hydroxide; In 1,4-dioxane; water; N,N-dimethyl-formamide;

DOI:10.1021/ol3024506

Reference yield:

cycl-isopropylidene malonate (2033-24-1) + C23H31NO5Si (1401229-70-6) → C25H31NO5Si

Guidance literature:

cycl-isopropylidene malonate; C₂₃H₃₁NO₅Si; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 6h;

In ethyl acetate; for 3h; Reflux;

DOI:10.1021/ol3024506

upstream raw materials:

tyrosine

benzyl chloroformate

Downstream raw materials:

C₁₇H₂₅NO₃Si

C₂₉H₄₅NO₄Si