(1R,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane

Base Information

Chemical Name:(1R,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane
CAS No.:1449741-26-7
Molecular Formula:C₂₆H₂₇NO₃
Molecular Weight:401.505
Hs Code.:

Synonyms:(1R,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane

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Chemical Property of (1R,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane

Chemical Property:

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Technology Process of (1R,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane

There total 3 articles about (1R,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449741-24-5
(1S,2R)-2-(triphenylmethoxy)methyl-1-(N-methoxy-N-methyl)carbamoyl-1-phenylsulfonylcyclopropane

: 1449741-25-6
(1S,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane

: 1449741-26-7
(1R,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane

Guidance literature:: With magnesium; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 1.16667h;
DOI:10.1016/j.bmc.2013.06.063

Reference yield:

: 409307-02-4
(1S,5R)-2-oxo-1-phenylsulfonyl-3-oxabicyclo[3.1.0]hexane

: 1449741-26-7
(1R,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane

Guidance literature:: Multi-step reaction with 2 steps

1.1: aluminum (III) chloride; triethylamine / dichloromethane / 5 h / 20 °C

1.2: 12 h / 20 °C

2.1: magnesium / methanol; tetrahydrofuran / 1.17 h / 0 - 20 °C

With aluminum (III) chloride; magnesium; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmc.2013.06.063

Reference yield:

: 76-83-5
trityl chloride

: 1449741-26-7
(1R,2S)-2-(triphenylmethoxymethyl)-1-(N-methoxy-N-methyl)carbamoylcycropropane

Guidance literature:: Multi-step reaction with 2 steps

1.1: aluminum (III) chloride; triethylamine / dichloromethane / 5 h / 20 °C

1.2: 12 h / 20 °C

2.1: magnesium / methanol; tetrahydrofuran / 1.17 h / 0 - 20 °C

With aluminum (III) chloride; magnesium; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmc.2013.06.063