1-[2-(4-NITROPHENYL)ETHYL]-1-AZONIABICYCLO[2.2.2]OCTANE BROMIDE

Base Information

• Chemical Name: 1-[2-(4-NITROPHENYL)ETHYL]-1-AZONIABICYCLO[2.2.2]OCTANE BROMIDE
• CAS No.: 73997-48-5
• Molecular Formula: Br*C₁₅H₂₁N₂O₂
• Molecular Weight: 341.248
• Hs Code.: 2933990090
• Mol file: 73997-48-5.mol

Synonyms:1-Azoniabicyclo[2.2.2]octane,1-[2-(4-nitrophenyl)ethyl]-, bromide (9CI)

Chemical Property of 1-[2-(4-NITROPHENYL)ETHYL]-1-AZONIABICYCLO[2.2.2]OCTANE BROMIDE

Chemical Property:

• PSA: 45.82000
• LogP: 0.25380

Purity/Quality:

98%Min ^*data from raw suppliers

1-[2-(4-NITROPHENYL)ETHYL]-1-AZONIABICYCLO[2.2.2]OCTANE BROMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[2-(4-NITROPHENYL)ETHYL]-1-AZONIABICYCLO[2.2.2]OCTANE BROMIDE

There total 1 articles about 1-[2-(4-NITROPHENYL)ETHYL]-1-AZONIABICYCLO[2.2.2]OCTANE BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Quinuclidine (100-76-5) + (4-nitrophenyl)ethyl bromide (5339-26-4) → N-(β-p-nitrophenylethyl)quinuclidinium bromide (73997-48-5)

Guidance literature:

In methanol; 1) 15 h, room temperature; 2) 50 deg C, 1 h;

DOI:10.1021/ja00526a047

Reference yield:

N-(β-p-nitrophenylethyl)quinuclidinium bromide (73997-48-5) → 4-nitrostyrene (100-13-0)

Guidance literature:

With acetohydroxamate buffer; potassium chloride; In water; at 25 - 40 ℃; Rate constant; Mechanism; Thermodynamic data; also with acetohydroxamic acid or KOH; also in D2O (isotope effect); also in the presence of EtOH and MeCN; ΔH(excit.), ΔS(excit.);

DOI:10.1021/ja00340a021

upstream raw materials:

Quinuclidine

(4-nitrophenyl)ethyl bromide

Downstream raw materials:

4-nitrostyrene