Technology Process of O6-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyxanthosine
There total 3 articles about O6-benzyl-3',5'-bis-O-(tert-butyldimethylsilyl)-2'-deoxyxanthosine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: PPh3; DEAD / dioxane
2: 67 percent / aq. acetic acid; NaNO2 / acetone / 4 h / 20 °C
With
acetic acid; triphenylphosphine; sodium nitrite; diethylazodicarboxylate;
In
1,4-dioxane; acetone;
1: Mitsunobu reaction;
DOI:10.1021/jo050847j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: imidazole / dimethylformamide
2: PPh3; DEAD / dioxane
3: 67 percent / aq. acetic acid; NaNO2 / acetone / 4 h / 20 °C
With
1H-imidazole; acetic acid; triphenylphosphine; sodium nitrite; diethylazodicarboxylate;
In
1,4-dioxane; N,N-dimethyl-formamide; acetone;
2: Mitsunobu reaction;
DOI:10.1021/jo050847j
- Guidance literature:
-
Multi-step reaction with 3 steps
1: imidazole / dimethylformamide
2: PPh3; DEAD / dioxane
3: 67 percent / aq. acetic acid; NaNO2 / acetone / 4 h / 20 °C
With
1H-imidazole; acetic acid; triphenylphosphine; sodium nitrite; diethylazodicarboxylate;
In
1,4-dioxane; N,N-dimethyl-formamide; acetone;
2: Mitsunobu reaction;
DOI:10.1021/jo050847j
